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NO. Products Name Types Items BP quality control specification Chp quality control specification
397 Valerian Dry Hydroalcoholic Extract IDENTIFICATION Thin-layer chromatography acetoxyvalerenic acid;valerenic acid
TESTS Water ≤5.0%
ASSAY Content ≥0.25% of sesquiterpenic acids, expressed as valerenic acid (C15H22O2 ; Mr 234.3) (anhydrous extract)
398 Valerian Tincture IDENTIFICATION Thin-layer chromatography acetoxyvalerenic acid;valerenic acid
TESTS Ethanol 95 to 105 % of the quantity stated on the label.
ASSAY Content ≥0.015 per cent m/m of sesquiterpenic acids, expressed as valerenic acid (C15H22O2 ; Mr 234.3).
399 Verbena Herb IDENTIFICATION Microscopic examination powder powder
Thin-layer chromatography Verbenin
TESTS
Total ash ≤10.0% ≤12.0%
Ash insoluble in hydrochloric acid ≤2.0% ≤4.0%
ASSAY Content ≥ 1.5 % of verbenalin (C17H24O10; Mr 388.4) (dried drug). ≥ 0.3 % of Oleic acid and ursolic acid
402 White Horehound IDENTIFICATION Microscopic examination powder
Thin-layer chromatography hydrochloric acid
TESTS Loss on drying ≤10.0%
Total ash ≤15.0%
Ash insoluble in hydrochloric acid ≤3.0%
ASSAY Content ≥ 0.7 % marrubiin (C20H28O4 ; Mr 332.4) (dried drug).
403 White Peony Root IDENTIFICATION Microscopic examination powder powder
Thin-layer chromatography paeoniflorin paeoniflorin
TESTS Loss on drying ≤12.0% ≤14.0%
Total ash ≤4.0% ≤4.0%
Ash insoluble in hydrochloric acid ≤0.5%
Pb, Cr, As, Hg and Cu ≤ 5mg/kg;≤ lmg/kg;≤ 2mg/kg; ≤ 0.2mg/kg;≤ 20mg/kg
ASSAY Content ≥1.6% of of paeoniflorin (C23H28O11; Mr 480.5) (dried drug). ≥1.6% of of paeoniflorin (C23H28O11; Mr 480.5) (dried drug).
Water-soluble extractive ≥22.0%
404 Wild Pansy IDENTIFICATION Microscopic examination powder
Thin-layer chromatography rutoside trihydrate R,hyperoside R,caffeic acid R
TESTS Foreign matter ≤3%
Swelling index ≤9
Loss on drying ≤12.0%
Total ash ≤15.0%
ASSAY Content ≥1.5% of flavonoids, expressed as violanthin (C27H30O14; Mr 578.5) (dried drug).
405 Wild Thyme IDENTIFICATION Microscopic examination powder
Thin-layer chromatography rutoside trihydrate R and rosmarinic acid R
TESTS Foreign matter ≤3% determined on 30 g.
Loss on drying ≤10.0%
Total ash ≤10.0%
Ash insoluble in hydrochloric acid ≤3.0%
ASSAY essential oil ≥3.0 mL/kg
406 Willow Bark IDENTIFICATION Microscopic examination powder
Thin-layer chromatography salicin R and chlorogenic acid R
TESTS Foreign matter ≤3%twigs with a diameter greater than 10 mm and maximum 2 %of other foreign matter.
Cadmium ≤2 ppm
Loss on drying ≤11.0%
Total ash ≤10.0%
ASSAY Content ≥1.5 % of total salicylic derivatives, expressed as salicin (C13H18O7 ; Mr 286.3) (dried drug).
407 Willow Bark Dry Extract IDENTIFICATION Thin-layer chromatography salicin R and chlorogenic acid R
TESTS
ASSAY Content ≥5% total salicylic derivatives, expressed as salicin (C13H18O7 ; Mr 286.3) (dried extract).
408 Withania Somnifera Root IDENTIFICATION Microscopic examination powder
Thin-layer chromatography withaferin A, withanolide B and β-sitosterol
TESTS Ash ≤7.0%
Acid-insoluble ash ≤1.0%
Loss on drying ≤12.0%
ASSAY Content ≥ 0.01% withaferin A (C28H38O6 ) and not less than≥ 0.01% withanolide A (C29 H42O7 ).
409 Wormwood IDENTIFICATION Microscopic examination powder
Thin-layer chromatography methyl red R and resorcinol R
TESTS Foreign matter ≤5 % of stems with a diameter greater than 4 mm and 2 % of other foreign matter
Bitterness value ≥10000
Loss on drying ≤10.0 %
Total ash ≤12.0 %
Ash insoluble in hydrochloric acid ≤1.0 %
ASSAY essential oil ≥2 mL/kg
410 Yarrow IDENTIFICATION Microscopic examination powder
Thin-layer chromatography cineole R and guaiazulene R
TESTS Foreign matter ≤5 % of stems with a diameter greater than 3 mm and 2 % of other foreign matter.
Loss on drying ≤12.0 %
Total ash ≤10.0 %
Ash insoluble in hydrochloric acid ≤2.5 %
ASSAY essential oil minimum 2 mL/kg
Content proazulenes, expressed as chamazulene (C14H16; Mr 184.3): minimum 0.02 per cent (dried drug).
411 Zanthoxylum Bungeanum Pericarp IDENTIFICATION Microscopic examination powder powder
Thin-layer chromatography chlorogenic acid R and emodin R reference herb drug
TESTS Foreign matter ≤5 % of seeds and ≤2% of other foreign matter.
Water ≤100mL/kg
Total ash ≤8.0%
Ash insoluble in hydrochloric acid ≤1.5%
ASSAY Content 15 mL/kg of essential oil ≥1. 5%(ml/g)
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