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NO. | Products Name | Types | Items | BP quality control specification | Chp quality control specification |
397 | Valerian Dry Hydroalcoholic Extract | IDENTIFICATION | Thin-layer chromatography | acetoxyvalerenic acid;valerenic acid | |
TESTS | Water | ≤5.0% | |||
ASSAY | Content | ≥0.25% of sesquiterpenic acids, expressed as valerenic acid (C15H22O2 ; Mr 234.3) (anhydrous extract) | |||
398 | Valerian Tincture | IDENTIFICATION | Thin-layer chromatography | acetoxyvalerenic acid;valerenic acid | |
TESTS | Ethanol | 95 to 105 % of the quantity stated on the label. | |||
ASSAY | Content | ≥0.015 per cent m/m of sesquiterpenic acids, expressed as valerenic acid (C15H22O2 ; Mr 234.3). | |||
399 | Verbena Herb | IDENTIFICATION | Microscopic examination | powder | powder |
Thin-layer chromatography | Verbenin | ||||
TESTS | |||||
Total ash | ≤10.0% | ≤12.0% | |||
Ash insoluble in hydrochloric acid | ≤2.0% | ≤4.0% | |||
ASSAY | Content | ≥ 1.5 % of verbenalin (C17H24O10; Mr 388.4) (dried drug). | ≥ 0.3 % of Oleic acid and ursolic acid | ||
402 | White Horehound | IDENTIFICATION | Microscopic examination | powder | |
Thin-layer chromatography | hydrochloric acid | ||||
TESTS | Loss on drying | ≤10.0% | |||
Total ash | ≤15.0% | ||||
Ash insoluble in hydrochloric acid | ≤3.0% | ||||
ASSAY | Content | ≥ 0.7 % marrubiin (C20H28O4 ; Mr 332.4) (dried drug). | |||
403 | White Peony Root | IDENTIFICATION | Microscopic examination | powder | powder |
Thin-layer chromatography | paeoniflorin | paeoniflorin | |||
TESTS | Loss on drying | ≤12.0% | ≤14.0% | ||
Total ash | ≤4.0% | ≤4.0% | |||
Ash insoluble in hydrochloric acid | ≤0.5% | ||||
Pb, Cr, As, Hg and Cu | ≤ 5mg/kg;≤ lmg/kg;≤ 2mg/kg; ≤ 0.2mg/kg;≤ 20mg/kg | ||||
ASSAY | Content | ≥1.6% of of paeoniflorin (C23H28O11; Mr 480.5) (dried drug). | ≥1.6% of of paeoniflorin (C23H28O11; Mr 480.5) (dried drug). | ||
Water-soluble extractive | ≥22.0% | ||||
404 | Wild Pansy | IDENTIFICATION | Microscopic examination | powder | |
Thin-layer chromatography | rutoside trihydrate R,hyperoside R,caffeic acid R | ||||
TESTS | Foreign matter | ≤3% | |||
Swelling index | ≤9 | ||||
Loss on drying | ≤12.0% | ||||
Total ash | ≤15.0% | ||||
ASSAY | Content | ≥1.5% of flavonoids, expressed as violanthin (C27H30O14; Mr 578.5) (dried drug). | |||
405 | Wild Thyme | IDENTIFICATION | Microscopic examination | powder | |
Thin-layer chromatography | rutoside trihydrate R and rosmarinic acid R | ||||
TESTS | Foreign matter | ≤3% determined on 30 g. | |||
Loss on drying | ≤10.0% | ||||
Total ash | ≤10.0% | ||||
Ash insoluble in hydrochloric acid | ≤3.0% | ||||
ASSAY | essential oil | ≥3.0 mL/kg | |||
406 | Willow Bark | IDENTIFICATION | Microscopic examination | powder | |
Thin-layer chromatography | salicin R and chlorogenic acid R | ||||
TESTS | Foreign matter | ≤3%twigs with a diameter greater than 10 mm and maximum 2 %of other foreign matter. | |||
Cadmium | ≤2 ppm | ||||
Loss on drying | ≤11.0% | ||||
Total ash | ≤10.0% | ||||
ASSAY | Content | ≥1.5 % of total salicylic derivatives, expressed as salicin (C13H18O7 ; Mr 286.3) (dried drug). | |||
407 | Willow Bark Dry Extract | IDENTIFICATION | Thin-layer chromatography | salicin R and chlorogenic acid R | |
TESTS | |||||
ASSAY | Content | ≥5% total salicylic derivatives, expressed as salicin (C13H18O7 ; Mr 286.3) (dried extract). | |||
408 | Withania Somnifera Root | IDENTIFICATION | Microscopic examination | powder | |
Thin-layer chromatography | withaferin A, withanolide B and β-sitosterol | ||||
TESTS | Ash | ≤7.0% | |||
Acid-insoluble ash | ≤1.0% | ||||
Loss on drying | ≤12.0% | ||||
ASSAY | Content | ≥ 0.01% withaferin A (C28H38O6 ) and not less than≥ 0.01% withanolide A (C29 H42O7 ). | |||
409 | Wormwood | IDENTIFICATION | Microscopic examination | powder | |
Thin-layer chromatography | methyl red R and resorcinol R | ||||
TESTS | Foreign matter | ≤5 % of stems with a diameter greater than 4 mm and 2 % of other foreign matter | |||
Bitterness value | ≥10000 | ||||
Loss on drying | ≤10.0 % | ||||
Total ash | ≤12.0 % | ||||
Ash insoluble in hydrochloric acid | ≤1.0 % | ||||
ASSAY | essential oil | ≥2 mL/kg | |||
410 | Yarrow | IDENTIFICATION | Microscopic examination | powder | |
Thin-layer chromatography | cineole R and guaiazulene R | ||||
TESTS | Foreign matter | ≤5 % of stems with a diameter greater than 3 mm and 2 % of other foreign matter. | |||
Loss on drying | ≤12.0 % | ||||
Total ash | ≤10.0 % | ||||
Ash insoluble in hydrochloric acid | ≤2.5 % | ||||
ASSAY | essential oil | minimum 2 mL/kg | |||
Content | proazulenes, expressed as chamazulene (C14H16; Mr 184.3): minimum 0.02 per cent (dried drug). | ||||
411 | Zanthoxylum Bungeanum Pericarp | IDENTIFICATION | Microscopic examination | powder | powder |
Thin-layer chromatography | chlorogenic acid R and emodin R | reference herb drug | |||
TESTS | Foreign matter | ≤5 % of seeds and ≤2% of other foreign matter. | |||
Water | ≤100mL/kg | ||||
Total ash | ≤8.0% | ||||
Ash insoluble in hydrochloric acid | ≤1.5% | ||||
ASSAY | Content | 15 mL/kg of essential oil | ≥1. 5%(ml/g) |