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NO. Products Name Types Items BP quality control specification Chp quality control specification
141 Fleeceflower Root IDENTIFICATION Microscopic examination Powder
Thin-layer chromatography emodin，resveratrol
TESTS Loss on drying ≤ 10.0 %
Total ash ≤ 5.0 %
Ash insoluble in hydrochloric acid ≤ 2.0 %
ASSAY Content ≥ 1.0 % of 2,3,5,4′-tetrahydroxystilbene-2-O-β-D-glucoside (dried drug)
142 Forsythia Fruit IDENTIFICATION Microscopic examination Powder
High-performance thin-layer chromatography ursolic acid，forsythoside
TESTS Foreign matter ≤ 5 %
Loss on drying ≤ 10.0 %
Total ash ≤ 4.0 %
ASSAY Ethanol-soluble extractive -
Content ≥ 0.15 % of forsythoside A (dried drug)
143 Frangula Bark IDENTIFICATION Microscopic examination Powder
Thin-layer chromatography barbaloin
physiochemical identification The aqueous layer becomes reddish-violet.
TESTS Other species of Rhamnus; anthrones（Thin-layer chromatography） barbaloin
Foreign matter ≤ 1 %
Loss on drying ≤ 10.0 %
Total ash ≤ 6.0 %
ASSAY Content ≥ 7.0 % of glucofrangulins, expressed as glucofrangulin A(dried drug)
144 Fraxinus Chinensis Bark IDENTIFICATION Microscopic examination powder
Thin-layer chromatography Esculetin,Esculin
TESTS Loss on drying ≤ 12.0 %
Total ash ≤ 10.0 %
Ash insoluble in hydrochloric acid ≤ 2.0 %
ASSAY Content 1.0 per cent for the sum of esculetin (C9H6O4; Mr 178.1) and esculin (C15H16O9; Mr 340.3) (dried drug).
145 Fresh Bilberry IDENTIFICATION Microscopic examination crushed fresh fruit
Thin-layer chromatography bilberry dry extract
TESTS Foreign matter "≤ 2 %, with no fruit of Sambucus nigra present. Adulteration with S. nigra L. is indicated by the presence of glossy, violet-black, ovoid berries without the circular fold due to the calyx, and containing ≤ 4 seeds."
Loss on drying 80.0 % to 90.0 %
Total ash ≤ 0.6 %
ASSAY Content ≥ 0.30 % of anthocyanins, expressed as cyanidin 3-O-glucoside chloride (dried drug)
146 Fumitory IDENTIFICATION Microscopic examination powder
Thin-layer chromatography protopine hydrochloride，quinine
TESTS Cadmium ≤ 1.5 ppm
Loss on drying ≤ 12.0 %
Total ash ≤ 15.0 %
ASSAY Content ≥ 0.40 % of total alkaloids, expressed as protopine (dried drug)
147 Ganoderma IDENTIFICATION Microscopic examination powder powder
High-performance thin-layer chromatography oleanolic acid,ganoderic acid A -
Thin-layer chromatography psoralen,Isopsoralen
TESTS Loss on drying ≤ 17.0 % ≤ 17.0 %
Total ash ≤ 2.0 % ≤ 3.2%
ASSAY Content ≥ 0.3 % of total triterpene acids, expressed as ganoderic acid A (dried drug) "≥ 0.3 % of Triterpenes and sterols,expressed as Oleanolic acid;≥ 0.9 % of Ganoderma lucidum polysaccharide ,expressed as Anhydrous glucose "
148 Garlic Powder IDENTIFICATION Microscopic examination
Thin-layer chromatography alanine allicin
TESTS Starch No blue colour develops.
Loss on drying ≤7% ≤13%
Total ash ≤5% ≤2%
ASSAY allicin 1 mg of butylparahydroxybenzoate corresponds to 8.65 mg of allicin. ≥0.15%
149 Gastrodia Elata Rhizome IDENTIFICATION Microscopic examination powder
Thin-layer chromatography gastrodin， β-sitosterol
Chromatographic profile -
TESTS Loss on drying ≤ 12.0 %
Total ash ≤ 4.0 %
sulfur dioxide residue -
ASSAY Ethanol-soluble extractive -
Content ≥ 0.20 % of gastrodin (dried drug)
150 Gentian IDENTIFICATION Microscopic examination powder
Thin-layer chromatography hyperoside，phenazone
TESTS Other species of Gentiana（Thin-layer chromatography） hyperoside，phenazone
Loss on drying -
Total ash ≤ 6.0 %
Bitterness value ≥ 10 000
Ash insoluble in hydrochloric acid -
ASSAY Content -
Water-soluble extractive ≥ 33 %
151 Gentian Tincture IDENTIFICATION Microscopic examination powder
Thin-layer chromatography hyperoside，phenazone
TESTS Other species of Gentiana（Thin-layer chromatography） hyperoside，phenazone
Loss on drying -
Total ash ≤ 6.0 %
Bitterness value ≥ 10 000
Ash insoluble in hydrochloric acid
ASSAY Water-soluble extractive ≥ 33 %
Content Content
152 Ginger IDENTIFICATION Microscopic examination powder transection
Thin-layer chromatography citral，resorcinol 6- gingerol
TESTS Water ≤ 100 mL/kg -
Total ash ≤ 6.0 % ≤ 2.0 %
ASSAY Content ≥ 15 mL/kg of essential oil (anhydrous drug) ≥ 0.12 mL/g of essential oil
Content - C17H26O4≥ 0.050%，C19H30O4 and C21H34O4 ≥0. 040%
153 Ginkgo Leaf IDENTIFICATION Microscopic examination powder powder
Thin-layer chromatography chlorogenic acid ，rutoside trihydrate Ginkgolide A,Ginkgolide B,Ginkgolide C,Bilobalide
TESTS Foreign matter ≤ 5 % of stems and 2 % of other foreign matter ≤ 2 %
Loss on drying ≤ 11.0 % ≤ 12.0 %
Total ash ≤ 11.0 % ≤ 10.0 %
ASSAY Ethanol-soluble extractive - ≥ 25.0 %
Content ≥ 0.5 % of flavonoids, expressed as flavone glycosides (dried drug) "≥ 0.4 % ofTotal flavonol glycosides; C20H24O9、C20H24O10 and C20H24O11 ≥0. 25%
154 Ginseng IDENTIFICATION Microscopic examination powder powder，transection
Thin-layer chromatography aescin，arbutin ginsenosideRg1 ，Rb1 ，Rf ,Re;reference herb drug
TESTS Loss on drying ≤ 10.0 % ≤ 12.0 %
Total ash ≤ 7.0 % ≤ 5.0 %
Pb, Cr, As, Hg and Cu - ≤ 5mg/kg；≤ lmg/kg；≤ 2mg/kg； ≤ 0.2mg/kg；≤ 20mg/kg
Organochlorine pesticides residue - quintozene≤0.1mg/kg;Hexachlorobenzene≤0.1mg/kg;Heptachlor and Heptachlor epoxide≤0.05mg/kg;irans-Chlordane、cu-Chlordane and oxy-Chlordane≤0.1mg/kg;
ASSAY Content ≥ 0.40 % for the sum of ginsenosides Rg1 and Rb1 (dried drug) ≥ 0.27 % for the sum of ginsenosides Rg1 and Re;ginsenosides Rb1≥0.18%
155 Ginseng Dry Extract IDENTIFICATION Microscopic examination powder
Thin-layer chromatography ginseng dry extract
TESTS Loss on drying ≤ 7.0 %
ASSAY Content ≥ 4.0 % of the sum of ginsenosides Rb1, Rb2, Rc, Rd, Re, Rf, Rg1 and Rg2, expressed as ginsenoside Rb1 (dried extract).
156 Glehnia Littoralis Root IDENTIFICATION Microscopic examination powder transection
Thin-layer chromatography ursolic acid ，beta-amyrin
TESTS Foreign matter ≤ 2%
Loss on drying ≤ 11.0%
Total ash ≤ 5.0%
Acid-insoluble Ash ≤ 0.5%
ASSAY
188 Java Tea IDENTIFICATION Microscopic examination Powder
Thin-layer chromatography sinensetin，scopoletin
TESTS Foreign matter ≤ 5 % of stems with a diameter greater than 1 mm and ≤ 2 % of other foreign m
Loss on drying ≤ 11.0 %
Total ash ≤ 12.5 %
ASSAY Content ≥ 0.3 % of rosmarinic acid (dried drug)
190 Juniper IDENTIFICATION Chromatographic profile "The characteristic peaks in the chromatogram obtained with the test solution are similar in retention time to those in the chromatogram obtained with the reference solution"
Thin-layer chromatography α-terpineol ， terpinen-4-ol
TESTS Relative density 0.857 to 0.876
Refractive index 1.471 to 1.483.
Optical rotation -15 to -5
Peroxide value ≤ 20
Fatty oils and resinified essential oils It complies with the test for fatty oils and resinified essential oils
Chromatographic profile "Determine the percentage Content of the components. Disregard the peak due to trimethylpentane and peaks comprising less than 0.01 % of the total surface area. The percentages are within the following ranges: — α-pinene: 20 % to 50 %; — sabinene: ≤ 20 %; — β-pinene: 1.0 % to 12 %; — β-myrcene: 1.0 % to 35 %; — α-phellandrene: ≤ 1.0 %; — limonene: 2.0 % to 12 %; — terpinen-4-ol: 0.5 % to 10 %;— bornyl acetate: ≤ 2.0 %; — β-caryophyllene: ≤ 7.0 %"
ASSAY
193 Knotgrass IDENTIFICATION Microscopic examination powder
Thin-layer chromatography caffeic acid，chlorogenic acid，hyperoside
TESTS Foreign matter ≤ 2 % of roots and ≤ 2 % of other foreign matter
Loss on drying ≤ 10.0 %
Total ash ≤ 10.0 %
Ash insoluble in hydrochloric acid
ASSAY Ethanol-soluble extractive -
Content ≥ 0.30 % of flavonoids, expressed as hyperoside(dried drug)
194 Kudzuvine Root IDENTIFICATION Microscopic examination powder
Thin-layer chromatography puerarin，daidzin R
TESTS Foreign matter ≤ 5 %
Loss on drying ≤ 10.0 %
Total ash ≤ 7.0 %
Ash insoluble in hydrochloric acid ≤ 1.0 %
Pb, Cr, As, Hg and Cu
Ethanol-soluble extractive
ASSAY Content ≥ 6.5 % of total isoflavonoids, expressed as puerarin (C21H20O9; Mr 416.4) (dried drug), of which ≥ 45 % consists of puerarin.
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